High-temperature elemental analysis and pyrolysis techniques for stable isotope analysis

An innovative molybdenum column liner for oxygen and hydrogen stable isotope analysis by pyrolysis.

The most widely used method for pyrolysing samples for hydrogen or oxygen isotopic analysis involves heating them to greater than 1300 degrees C in a helium stream passed through a glassy carbon tube in an alumina casing. There are a number of difficulties with this. Glassy carbon tubes are expensive and interaction between the carbon tube and the outer casing produces unwanted carbon monoxide ...

Analytical Techniques for Elemental Analysis of Minerals

response articles: micro and macro analysis

the present study reports an analysis of response articles in four different disciplines in the social sciences, i.e., linguistics, english for specific purposes (esp), accounting, and psychology. the study has three phases: micro analysis, macro analysis, and e-mail interview. the results of the micro analysis indicate that a three-level linguistic pattern is used by the writers in order to cr...

A reactor for high-temperature pyrolysis and oxygen isotopic analysis of cellulose via induction heating.

A reactor for converting cellulose into carbon monoxide for subsequent oxygen isotopic analysis via continuous flow isotope ratio mass spectrometry is described. The system employs an induction heater to produce temperatures >or=1500 degrees C within a molybdenum foil crucible positioned by boron nitride (BN) spacers within a quartz outer sleeve. For samples of a homogeneous working standard ce...

Stable Isotope Analysis of Fossil Bone

The biological signal hidden in stable carbon, nitrogen, oxygen and strontium stable isotope ratios in archaeological and fossil skeletal finds give clues to a variety of palaeoecological parameters. In contrast to trace element analysis, these parameters can be assessed on the individual level, which is a major advantage for palaeoanthropology, where single finds prevail over multiple finds at...